By Satoru Shimomura, Sareeya Bureekaew, Susumu Kitagawa (auth.), Mir Wais Hosseini (eds.)
From the studies: “This e-book supplies an summary of a few contemporary advancements in crystal engineering of molecular and metalloorganic solids in 5, primarily self sufficient chapters written via varied authors. … All in all, this e-book makes solid studying fabric that may entice nonexperts via showcasing a few contemporary advancements within the box of crystal engineering, in addition to to … specialists looking an in depth review of a particular subfield, akin to a entire account of all attainable assemblies of bipyridine-dioxide … .” (Dmitrii F. Perepichka, magazine of the yank Chemical Society, Vol. 132 (11), 2010)
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Withersby MA, Blake AJ, Champness NR, Cooke PA, Hubberstey P, Realf AL, Schr¨oder M (2000) J Chem Soc Dalton Trans, p 3261 28. Rosi NL, Eddaoudi M, Kim J, O’Keeffe M, Yaghi OM (2002) CrystEngComm 4:401 29. Sui B, Fan J, Okamura T, Sun W-Y, Ueyama N (2005) Solid State Chem 7:969 30. Hill RJ, Long D-L, Champness NR, Hubberstey P, Schr¨oder M (2005) Acc Chem Res 38:337 31. Long D-L, Blake AJ, Champness NR, Wilson C, Schr¨oder M (2001) J Am Chem Soc 123:3401 32. Long D-L, Blake AJ, Champness NR, Wilson C, Schr¨oder M (2001) Angew Chem Int Ed 40:2444 33.
Therefore it is necessary to make sure that the scale-up from laboratory preparation to industrial production does not introduce variations in crystal form. Polymorph assessment also guarantees that the product conforms to the guidelines of the appropriate regulatory agencies and does not infringe the intellectual property protection that may cover other crystal forms [32]. D. Braga et al. Fig. 3 Some general relationships between polymorphs, solvates and amorphous phases and the type of research laboratory or industrial or process for preparation and interconversion: 1 crystallization; 2 desolvation; 3 exposure to solvent/vapour uptake; 4 freeze drying; 5 heating; 6 melting; 7 precipitation; 8 quench cooling; 9 milling; 10 spray drying; 11 kneading; 12 wet granulation.
9 Conclusions The scope of this review has not been that of providing the reader with a comprehensive coverage of the topic of crystal forms, rather we have aimed at an introductory view of the phenomena of multiple crystals forms in general, and polymorphism in particular. g. theo- Crystal Polymorphism and Multiple Crystal Forms retical methods to study polymorphism), in particular the computational exploration of the possible crystalline structures of a given molecule. The interested reader will find in the necessarily limited number of references a good starting point for further reading.